Low% recovery of checked standard

CN
CN
in Instrumentation and Mass Spectrometry
<p><span>What is the possible problem if I have a low % recovry of checked standard?</span></p><p><span>I also have a high % RSD standard of 6 injections.</span></p><p><span>Please advice</span></p><p><span>Thank you</span></p><p><span>CN</span></p>

Answers

  • lizh
    lizh

    Hello:

    It is possible the reproducibility issue is causing the recovery issue, or they could be unrelated, please take a look at the BJ thread this can give you some background on recovery issues, could be very similar. Plaese send a chromatogram if possible and Method details such as the mobile phase, injection mode, washes and injection volume.

    Many TX

    Liz

  • C_Hand
    C_Hand

    Hello,

    By BJ Thread, I believe Liz is referring to a previous discussion posted by "BJ" entitled "%area of related compounds depending on the injection technique"

    Hope this helps,

    Christine

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